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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">kaz65</journal-id><journal-title-group><journal-title xml:lang="ru">Почвоведение и агрохимия</journal-title><trans-title-group xml:lang="en"><trans-title>Soil Science and Agrichemistry</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1999-740X</issn><issn pub-type="epub">2959-3433</issn><publisher><publisher-name>Казахский научно-исследовательский институт почвоведения и агрохимии имени У.У. Успанова</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">0.51886/1999-740X_2021_2_62</article-id><article-id custom-type="elpub" pub-id-type="custom">kaz65-25</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>Обзорная статья</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>Review</subject></subj-group></article-categories><title-group><article-title>ЗЕЛЕНЫЕ МЕТОДИКИ АНАЛИЗА ПЕСТИЦИДОВ В ЗЕРНОВЫХ КУЛЬТУРАХ: ОБЗОР</article-title><trans-title-group xml:lang="en"><trans-title>GREEN METHODS OF ANALYSIS OF PESTICIDES IN CEREALS: OVERVIEW</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Мамедова</surname><given-names>М. Р.</given-names></name><name name-style="western" xml:lang="en"><surname>Mamedova</surname><given-names>M. R.</given-names></name></name-alternatives><bio xml:lang="ru"><p>050060, г. Алматы, пр-т аль-Фараби, 71</p></bio><bio xml:lang="en"><p>050070, Almaty, al-Farabi Ave, 71</p></bio><email xlink:type="simple">mamedova.madina@kaznu.kz</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Ибраимов</surname><given-names>А. Б.</given-names></name><name name-style="western" xml:lang="en"><surname>Ibraimov</surname><given-names>A. B.</given-names></name></name-alternatives><bio xml:lang="ru"><p>050060, г. Алматы, пр-т аль-Фараби, 71</p></bio><bio xml:lang="en"><p>050070, Almaty, al-Farabi Ave, 71</p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Кунанов</surname><given-names>А. Н.</given-names></name><name name-style="western" xml:lang="en"><surname>Kunanov</surname><given-names>A. N.</given-names></name></name-alternatives><bio xml:lang="ru"><p>050060, г. Алматы, пр-т аль-Фараби, 71</p></bio><bio xml:lang="en"><p>050070, Almaty, al-Farabi Ave, 71</p></bio><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Алимжанова</surname><given-names>М. Б.</given-names></name><name name-style="western" xml:lang="en"><surname>Alimzhanova</surname><given-names>M. B.</given-names></name></name-alternatives><bio xml:lang="ru"><p>050060, г. Алматы, пр-т аль-Фараби, 71</p></bio><bio xml:lang="en"><p>050070, Almaty, al-Farabi Ave, 71</p></bio><xref ref-type="aff" rid="aff-3"/></contrib><contrib contrib-type="author" corresp="yes"><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Тукенова</surname><given-names>З. А.</given-names></name><name name-style="western" xml:lang="en"><surname>Tukenova</surname><given-names>Z. A.</given-names></name></name-alternatives><bio xml:lang="ru"><p>050070, г.Алматы, пр-т аль-Фараби, 75 В</p></bio><bio xml:lang="en"><p>050060, Almaty, al-Farabi Ave, 75 В</p></bio><xref ref-type="aff" rid="aff-4"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru">Казахский национальный университет им. аль-Фараби, физико-технический факультет<country>Казахстан</country></aff><aff xml:lang="en">al-Farabi Kazakh National University, Faculty of Physics and Technology<country>Kazakhstan</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru">Казахский национальный университет им. Аль-Фараби, химико-технологический факультет<country>Казахстан</country></aff><aff xml:lang="en">al-Farabi Kazakh National University, Faculty of Chemistry and Chemical Technology<country>Kazakhstan</country></aff></aff-alternatives><aff-alternatives id="aff-3"><aff xml:lang="ru">Казахский национальный университет им. аль-Фараби, физико-технический факультет; Казахский национальный университет им. Аль-Фараби, химико-технологический факультет<country>Казахстан</country></aff><aff xml:lang="en">al-Farabi Kazakh National University, Faculty of Physics and Technology; al-Farabi Kazakh National University, Faculty of Chemistry and Chemical Technology<country>Kazakhstan</country></aff></aff-alternatives><aff-alternatives id="aff-4"><aff xml:lang="ru">ТОО Казахский научно-исследовательский институт почвоведения и агрохимии им. У.У. Успанова<country>Казахстан</country></aff><aff xml:lang="en">LLP Kazakh U.U. Uspanov Research Institute of Soil Science and Agricultural Chemistry<country>Kazakhstan</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2021</year></pub-date><pub-date pub-type="epub"><day>08</day><month>08</month><year>2022</year></pub-date><volume>0</volume><issue>2</issue><fpage>62</fpage><lpage>79</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Мамедова М.Р., Ибраимов А.Б., Кунанов А.Н., Алимжанова М.Б., Тукенова З.А., 2022</copyright-statement><copyright-year>2022</copyright-year><copyright-holder xml:lang="ru">Мамедова М.Р., Ибраимов А.Б., Кунанов А.Н., Алимжанова М.Б., Тукенова З.А.</copyright-holder><copyright-holder xml:lang="en">Mamedova M.R., Ibraimov A.B., Kunanov A.N., Alimzhanova M.B., Tukenova Z.A.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://journal.soil.kz/jour/article/view/25">https://journal.soil.kz/jour/article/view/25</self-uri><abstract><p>Пестициды используются во всем мире, начиная с середины XX века, для производства зерновых культур и их производных в сельском хозяйстве. Многие пестициды, особенно фунгициды и инсектициды, используются для предотвращения различных заболевании и повышения урожайности во время созревания. Поступление пестицидов в окружающую среду составляет долю одного процента от общего количества химических загрязнителей, но, учитывая, что эти соединения нацелены на подавление определенных групп организмов, пестициды и продукты их трансформации оказывают токсическое воздействие на здоровье человека, попадая в организм с овощами и фруктами, в том числе с их поверхности, если плоды плохо вымыты и на различные формы биоты. А также, из злаков, так как они могут всасываться в них из почвы. Безопасных пестицидов не существует, даже при использовании в малых количествах они могут вызывать различные аллергические реакции и отравления. При производстве сельскохозяйственной продукции используются одобренные пестициды, но это не отменяет того факта, что у длительного использования препарата могут быть негативные последствия. Следовательно, постоянный мониторинг остаточного количества пестицидов в этих продуктах снижает риск для здоровья человека и окружающей среды. Поэтому необходимы эффективные, экспрессные и экономически выгодные методики определения остаточных количеств пестицидов. В статье отражены методы подготовки проб при анализе пестицидов в зерновых культурах, а также особенности метода твердофазной микроэкстракции одной из методов экологической, зеленой химии при подготовке проб.</p></abstract><trans-abstract xml:lang="en"><p>Pesticides have been used all over the world since the mid-twentieth century to protect cereals and their derivatives in agriculture from pests, insects and fungi. The release of pesticides into the environment makes up a fraction of one percent of the total amount of chemical pollutants, but given that these compounds are aimed at suppressing certain groups of organisms, pesticides and their transformation products have a toxic effect on various forms of biota and on human health when ingested with vegetables and fruits, including from their surface, if they are poorly washed. And also, from cereals, as they can be absorbed into them from the soil. There are no safe pesticides, even when used in small quantities, they can cause various allergic reactions and poisoning. In the production of agricultural products, approved pesticides are used, but this does not negate the fact that long-term use of the drug can have negative consequences. Therefore, constant monitoring of the residual amount of pesticides in these products reduces the risk to human health and the environment. Hence, there is a need for efficient, rapid and cost-effective methods for the determination of pesticide residues. The article reflects the methods of sample preparation in the analysis of pesticides in grain crops, as well as features of the method of solid-phase micro extraction of one of the methods of environmental, green chemistry in the preparation of samples.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>злаки</kwd><kwd>пестициды</kwd><kwd>методы пробоподготовки</kwd><kwd>метод твердофазной микроэкстракции</kwd><kwd>хроматография</kwd></kwd-group><kwd-group xml:lang="en"><kwd>cereals</kwd><kwd>pesticides</kwd><kwd>methods of sample preparation</kwd><kwd>solid-phase micro extraction method</kwd><kwd>chromatography</kwd></kwd-group><funding-group xml:lang="en"><funding-statement>This work was conducted under the project AP08857501 «Improvement and development of highly sensitive methods for ensuring food safety in Kazakhstan» funded by the Ministry of Education and Science of Kazakhstan from 2020 to 2022.</funding-statement></funding-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Sharma D., Nagpal A., Pakade Y. 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